![](/CAS/GIF/101947-16-4.gif)
1H,1H,2H,2H-Perfluorodecyltriethoxysilane synthesis
- Product Name:1H,1H,2H,2H-Perfluorodecyltriethoxysilane
- CAS Number:101947-16-4
- Molecular formula:C16H19F17O3Si
- Molecular Weight:610.38
![1H,1H,2H,2H-Perfluorodecyltriethoxysilane 1H,1H,2H,2H-Perfluorodecyltriethoxysilane](/NewsImg/2023-11-13/6383548885471378484597420.jpg)
![Triethoxysilane](/CAS/GIF/998-30-1.gif)
998-30-1
239 suppliers
$30.00/25 g
![1H,1H,2H-Perfluoro-1-decene](/CAS/GIF/21652-58-4.gif)
21652-58-4
197 suppliers
$12.00/5g
![1H,1H,2H,2H-Perfluorodecyltriethoxysilane](/CAS/GIF/101947-16-4.gif)
101947-16-4
311 suppliers
$5.00/250mg
Yield:101947-16-4 97.3%
Reaction Conditions:
with chloroplatinic acid in isopropyl alcohol at 25; for 0.115 h;
Steps:
2 Example 2
An isopropyl alcohol solution of chloroplatinic acid is disposed at a concentration of 10 mmol/L. The mixed reaction module M having a preset temperature of 25 ° C was flowed through the material passage C through the metering pump P3 at a flow rate of 7 ml/min. At the same time, perfluorooctylethylene is passed through channel A, The metering pump P1 is fed into the mixed reaction module M at a preset temperature of 25 ° C at a flow rate of 6 ml/min; and the triethoxysilane is passed through the channel B at the same time. The metering pump P2 was supplied to the mixed reaction module M having a preset temperature of 25 ° C at a flow rate of 4.2 ml/min. After staying in the mixed reaction module M for 6.9 minutes, it flows out.The reaction liquid flowing out from the outlet D was collected in a single-necked flask. The volatile matter is removed by distillation under reduced pressure. Finally, 1H, 1H, 2H, 2H-perfluorodecyltriethoxysilane with a purity of 99% is obtained. The yield can reach 97.3%.
References:
Shandong Cathay Shenzhou New Materials Co., Ltd.;Wang Hanli;Bi Congcong;Wang Lei;Wang Jun CN109535195, 2019, A Location in patent:Paragraph 0043; 0044