1H-Imidazole, 5-(bromomethyl)-1-ethyl- synthesis
- Product Name:1H-Imidazole, 5-(bromomethyl)-1-ethyl-
- CAS Number:1256561-80-4
- Molecular formula:C6H9BrN2
- Molecular Weight:189.05
215872-62-1
46 suppliers
$36.00/100mg
1256561-80-4
2 suppliers
inquiry
Yield:-
Reaction Conditions:
with phosphorus tribromide in dichloromethane at 20; for 6 h;
Steps:
78
To a solution of (1 -ethyl- lH-imidazol-5-yl)methanol (631 mg, 5.0 mmol) in dichloromethane (20 niL) was added dropwise tribromophosphane (0.94 mL, 10.0 mmol). The resulting mixture was stirred at room temperature for 6 hours.
References:
WO2010/132999,2010,A1 Location in patent:Page/Page column 131