ChemicalBook CAS DataBase List 5-Bromo-2,3-dihydro-1H-inden-1-amine

5-Bromo-2,3-dihydro-1H-inden-1-amine synthesis

4synthesis methods

Product Name:5-Bromo-2,3-dihydro-1H-inden-1-amine
CAS Number:185122-74-1
Molecular formula:C9H10BrN
Molecular Weight:212.09

To a solution of 5-bromo-2,3-dihydro-1H-inden-1-one (100 g, 474 mmol, 1.00 equiv) in methanol (1.5 L) was added ammonium formate (300 g, 4.76 mol, 10.0 equiv). After stirring for 1 h, NaBH3CN (90 g, 1.43 mol, 3.02 equiv) was added. The mixture was heated at 60 ℃ for 2 h, concentrated under reduced pressure, and purified by silica gel chromatography (EA/PE, 1/10) to afford 64 g (64%) of 5-Bromo-2,3-dihydro-1H-inden-1-amine as a brown solid.
1H-INDEN-1-AMINE, 5-BROMO-2,3-DIHYDRO-

34598-49-7 Synthesis

34598-49-7
365 suppliers
$14.00/5g

185122-74-1
56 suppliers
$98.00/50mg

Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-

1000210-73-0
0 suppliers
inquiry

185122-74-1
56 suppliers
$98.00/50mg

References

185122-63-8
10 suppliers
$90.00/1g

185122-74-1
56 suppliers
$98.00/50mg

References

1000210-73-0
0 suppliers
inquiry

185122-74-1
56 suppliers
$98.00/50mg

References

5-Bromo-2,3-dihydro-1H-inden-1-amine Related Search:

5-bromo-2,4-dimethylphenylamine