1H-Pyrazole,4-methyl-1-nitro-(9CI) synthesis
- Product Name:1H-Pyrazole,4-methyl-1-nitro-(9CI)
- CAS Number:38858-82-1
- Molecular formula:C4H5N3O2
- Molecular Weight:127.1
7554-65-6
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Yield:38858-82-1 79%
Reaction Conditions:
with tert.-butylnitrite;ammonium cerium (IV) nitrate;oxygen in acetonitrile at 100; for 16 h;Inert atmosphere;Schlenk technique;
References:
Yang, Tao;Li, Xiaoqian;Deng, Shuang;Qi, Xiaotian;Cong, Hengjiang;Cheng, Hong-Gang;Shi, Liangwei;Zhou, Qianghui;Zhuang, Lin [Journal of the American Chemical Society,2022,vol. 2,# 9,p. 2152 - 2161] Location in patent:supporting information