ChemicalBook CAS DataBase List 2-(1-Adamantyl)oxirane

2-(1-Adamantyl)oxirane synthesis

7synthesis methods

Product Name:2-(1-Adamantyl)oxirane
CAS Number:28173-62-8
Molecular formula:C12H18O
Molecular Weight:178.27

5122-82-7 Synthesis

5122-82-7
108 suppliers
$45.00/10mg

28173-62-8
15 suppliers
$45.00/50mg

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 87 percent / NaBH₄, 0.5percent NaOH / propan-2-ol / 1.) from 20 deg C to 25 deg C, 3 h, 2.) from 60 deg C to 70 deg C, 30 min
2: aq. NaOH / propan-2-ol / 1 h / 35 - 40 °C

References:

Shiryaev, A. K.;Moiseev, I. K.;Boreko, E. I.;Korobchenko, L. V.;Vladyko, G. V. [Pharmaceutical Chemistry Journal,1990,vol. 24,# 5,p. 339 - 343][Khimiko-Farmatsevticheskii Zhurnal,1990,vol. 24,# 5,p. 23 - 25]