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2,2'-(5-broMo-1,3-phenylene)dipyridine synthesis

9synthesis methods
-

Yield:150239-89-7 70%

Reaction Conditions:

with copper(l) iodide;tetrakis(triphenylphosphine) palladium(0);potassium hydroxide in 1,2-dimethoxyethane; for 20 h;Reflux;Suzuki coupling;

References:

Wadman, Sipke H.;Tooke, Duncan M.;Spek, Anthony L.;van Klink, Gerard P.M.;van Koten, Gerard [Inorganica Chimica Acta,2010,vol. 363,# 8,p. 1701 - 1706] Location in patent:experimental part