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ChemicalBook CAS DataBase List 2,2'-DICHLORO-[3,4']-BIPYRIDINE

2,2'-DICHLORO-[3,4']-BIPYRIDINE synthesis

2synthesis methods
78607-36-0 Synthesis
2-Chloro-3-iodopyridine

78607-36-0
352 suppliers
$14.00/1g

458532-96-2 Synthesis
2-Chloro-4-pyridylboronic acid

458532-96-2
263 suppliers
$6.00/250mg

-

Yield:643082-10-4 66%

Reaction Conditions:

with sodium carbonate;tetrakis(triphenylphosphine) palladium(0) in 1,4-dioxane;water; for 18 h;Heating;Suzuki cross-coupling;

References:

Bouillon, Alexandre;Voisin, Anne Sophie;Robic, Audrey;Lancelot, Jean-Charles;Collot, Valerie;Rault, Sylvain [Journal of Organic Chemistry,2003,vol. 68,# 26,p. 10178 - 10180]