2-(2-Nitrophenyl)pyridine synthesis
- Product Name:2-(2-Nitrophenyl)pyridine
- CAS Number:4253-81-0
- Molecular formula:C11H8N2O2
- Molecular Weight:200.19
1008-89-5
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Yield:4253-81-0 88%
Reaction Conditions:
with dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer;[hydroxy(tosyloxy)iodo]benzene;acetic acid;sodium nitrite in acetone at 80; for 16 h;Sealed tube;Molecular sieve;regioselective reaction;Reagent/catalyst;Temperature;
References:
Xie, Fang;Qi, Zisong;Li, Xingwei [Angewandte Chemie - International Edition,2013,vol. 52,# 45,p. 11862 - 11866][Angew. Chem.,2013,vol. 125,# 45,p. 12078 - 12082,5] Location in patent:supporting information
