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18162-48-6872-50-4Methylene ChloridenaphthaleneTHFTitanium Dioxide

2',3',4',6'-TETRAMETHOXYACETOPHENONE synthesis

13synthesis methods
Preparation by reaction of acetyl chloride with 1,2,3,5-tetramethoxybenzene (m.p. 47°), in the presence of aluminium chloride.
1-(2-hydroxy-3,4,6-trimethoxy-phenyl)ethanone

7507-98-4
4 suppliers
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Iodomethane

74-88-4
340 suppliers
$15.00/10g

2',3',4',6'-TETRAMETHOXYACETOPHENONE

7508-05-6
14 suppliers
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Yield:7508-05-6 94%

Reaction Conditions:

with potassium carbonate in N,N-dimethyl-formamide at 60; for 1.5 h;Inert atmosphere;

References:

Asakawa, Tomohiro;Hiza, Aiki;Nakayama, Miho;Inai, Makoto;Oyama, Dai;Koide, Hiroyuki;Shimizu, Kosuke;Wakimoto, Toshiyuki;Harada, Norihiro;Tsukada, Hideo;Oku, Naoto;Kan, Toshiyuki [Chemical Communications,2011,vol. 47,# 10,p. 2868 - 2870] Location in patent:supporting information; experimental part

1,2,3,5-TETRAMETHOXYBENZENE

5333-45-9
33 suppliers
$240.00/10g

75-36-5 Synthesis
Acetyl chloride

75-36-5
564 suppliers
$17.92/100G

2',3',4',6'-TETRAMETHOXYACETOPHENONE

7508-05-6
14 suppliers
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References
1-(2-hydroxy-3,4,6-trimethoxy-phenyl)ethanone

7507-98-4
4 suppliers
inquiry

Dimethyl sulfate

77-78-1
286 suppliers
$22.00/25g

2',3',4',6'-TETRAMETHOXYACETOPHENONE

7508-05-6
14 suppliers
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References
1,2,3,5-TETRAMETHOXYBENZENE

5333-45-9
33 suppliers
$240.00/10g

Acetic anhydride

108-24-7
5 suppliers
$14.00/250ML

2',3',4',6'-TETRAMETHOXYACETOPHENONE

7508-05-6
14 suppliers
inquiry

References
530-55-2 Synthesis
2,6-DIMETHOXY-1,4-BENZOQUINONE

530-55-2
132 suppliers
$23.50/1g

2',3',4',6'-TETRAMETHOXYACETOPHENONE

7508-05-6
14 suppliers
inquiry

References

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