ChemicalBook CAS DataBase List 2,3-DIBROMOPHENOL

2,3-DIBROMOPHENOL synthesis

6synthesis methods

Product Name:2,3-DIBROMOPHENOL
CAS Number:57383-80-9
Molecular formula:C6H4Br2O
Molecular Weight:251.9

583-53-9
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$10.00/5g

57383-80-9
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$125.00/50 mg

Yield: 95%

Reaction Conditions:

with tert.-butylhydroperoxide;copper acetylacetonate in water at 20; for 12 h;Time;

Steps:

1-3 Example 3:
Add o-dibromobenzene (1.0 mmol), tBuOOH (1.4 mmol), andCu (acac) 2 (0.10mmol), then add 2mL of solvent water, and react at room temperature for 12 hours,After the reaction was completed, the reaction solution was concentrated, and the corresponding product was obtained by column chromatography. The isolated yield was 95%.

References:

Shanghai Institute of Technology;Yao Zijian;Qiao Xinchao CN110981702, 2020, A Location in patent:Paragraph 0020-0028