2,3-DIHYDRO-2,2-DIMETHYL-6-FLUORO-1H-INDEN-1-ONE synthesis
- Product Name:2,3-DIHYDRO-2,2-DIMETHYL-6-FLUORO-1H-INDEN-1-ONE
- CAS Number:198341-10-5
- Molecular formula:C11H11FO
- Molecular Weight:178.2
1481-32-9
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Yield:198341-10-5 85%
Reaction Conditions:
Stage #1: 6-fluoroindan-1-onewith sodium hydride in tetrahydrofuran;mineral oil at 0; for 0.5 h;Inert atmosphere;
Stage #2: methyl iodide in tetrahydrofuran;mineral oil at 0 - 20;Inert atmosphere;
References:
Chen, Jun;Shi, Zhan;Lu, Ping [Organic Letters,2021,vol. 23,# 19,p. 7359 - 7363] Location in patent:supporting information
1481-32-9
234 suppliers
$5.00/250mg
198341-10-5
1 suppliers
inquiry