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ChemicalBook CAS DataBase List 2,4,5-Trichlorobenzoic acid

2,4,5-Trichlorobenzoic acid synthesis

13synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 97 percent / 1a) AlCl3, 1b) AlCl3 / 1a) 8 h, r.t., 1b) 16 h, -10 deg C
2: 1) 30percent Oleum, 2) ice / 1) 100 deg C, 24 h

References:

Castaner, J.;Riera, J.;Carilla, J.;Robert, A.;Molins, E.;Miravitlles, C. [Journal of Organic Chemistry,1991,vol. 56,# 1,p. 103 - 110]

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