ChemicalBook CAS DataBase List 2,4-Hexadienal

2,4-Hexadienal synthesis

13synthesis methods

Product Name:2,4-Hexadienal
CAS Number:80466-34-8
Molecular formula:C6H8O
Molecular Weight:96.13

50-00-0 Synthesis

50-00-0
843 suppliers
$10.00/25g

75-07-0 Synthesis

75-07-0
414 suppliers
$14.00/5mL

80466-34-8
16 suppliers
inquiry

40650-87-1
16 suppliers
$219.00/25 mg

107-02-8
4 suppliers
$38.60/4s8501

123-73-9
193 suppliers
$40.00/5g

Yield: 22% ， 14% ， 7% ， 6%

Reaction Conditions:

with N-(benzoyl)-L-proline in N,N-dimethyl acetamide at 125; for 3 h;Autoclave;Aldol Condensation;

Steps:

General procedure: The experiments were carried out in static steel and glass thick-walled autoclaves (Aldrich) at 25 and 125°C for 3 and 24 h, respectively. Water, toluene, N,N'-dimethylacetamide (DMAA) were used as a solvent. A weighed amount of a solvent was placed into the autoclave, a required amount of an aldehyde was added, and a catalyst was introduced into the obtained solution. The process is accompanied by the change in the color of the reaction solution from pale yellow to black depending on the catalytic system used.

References:

Martsinkevich;Bruk;Dashko;Afaunov;Flid;Sedov [Petroleum Chemistry,2018,vol. 58,# 12,p. 1032 - 1035][Neftekhimiya,2018,vol. 58,# 6,p. 686 - 689,4]