2-{[(4-methylphenyl)sulfonyl]methyl}pyridine synthesis

5synthesis methods

Product Name:2-{[(4-methylphenyl)sulfonyl]methyl}pyridine
CAS Number:58414-96-3
Molecular formula:C13H13NO2S
Molecular Weight:247.3128

824-79-3 Synthesis

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2-{[(4-methylphenyl)sulfonyl]methyl}pyridine

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Yield:-

Steps:

Multi-step reaction with 4 steps
1: N,N-dimethyl-formamide / 12 h / 25 °C / Inert atmosphere
2: caesium carbonate / acetonitrile / 4 h / 25 °C
3: (triphenylphosphine)gold(I) chloride; silver hexafluoroantimonate / dichloromethane / 1 h / 25 °C / Inert atmosphere
4: potassium hydroxide / methanol / Reflux

References:

Undeela, Sridhar;Thadkapally, Srinivas;Nanubolu, Jagadeesh Babu;Singarapu, Kiran Kumar;Menon, Rajeev S. [Chemical Communications,2015,vol. 51,# 72,p. 13748 - 13751]