2,5-DIMETHYLBENZOTHIOPHENE synthesis
- Product Name:2,5-DIMETHYLBENZOTHIOPHENE
- CAS Number:16587-48-7
- Molecular formula:C10H10S
- Molecular Weight:162.25
14315-14-1
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74-88-4
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$15.00/10g
16587-48-7
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$505.80/5MG
Yield:16587-48-7 98%
Reaction Conditions:
Stage #1: 5-methylthianaphthenewith n-butyllithium in tetrahydrofuran;hexane at -78; for 0.5 h;Inert atmosphere;
Stage #2: methyl iodide in tetrahydrofuran;hexane at -78 - 20; for 2 h;Inert atmosphere;
References:
Shigeno, Masanori;Sasaki, Keita;Nozawa-Kumada, Kanako;Kondo, Yoshinori [Organic Letters,2019,vol. 21,# 12,p. 4515 - 4519] Location in patent:supporting information
53299-60-8
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16587-48-7
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$505.80/5MG
14422-07-2
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16587-48-7
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106-45-6
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$10.00/1g
16587-48-7
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108237-58-7
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16587-48-7
12 suppliers
$505.80/5MG