2-(5-PHENYLOXAZOL-2-YL)PHENOL synthesis

7synthesis methods

Product Name:2-(5-PHENYLOXAZOL-2-YL)PHENOL
CAS Number:103656-73-1
Molecular formula:C15H11NO2
Molecular Weight:237.25

64908-64-1 Synthesis

64908-64-1
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103656-73-1
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Yield:-

Steps:

Multi-step reaction with 3 steps
1: hydrazine hydrate / methanol; chloroform / 20 °C / Inert atmosphere
2: sodium carbonate / ethyl acetate; water / 2 h / 0 °C / Inert atmosphere
3: dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; silver hexafluoroantimonate; Trimethylacetic acid; cesium pivalate; silver carbonate / N,N-dimethyl-formamide / 24 h / 140 °C / Inert atmosphere; Schlenk technique

References:

Li, Bijin;Lan, Jingbo;Wu, Di;You, Jingsong [Angewandte Chemie - International Edition,2015,vol. 54,# 47,p. 14008 - 14012][Angew. Chem.,2016]

5468-37-1 Synthesis