2,8-Quinolinediol synthesis
- Product Name:2,8-Quinolinediol
- CAS Number:15450-76-7
- Molecular formula:C9H7NO2
- Molecular Weight:161.16
6889-84-5
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15450-76-7
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Yield:15450-76-7 85%
Reaction Conditions:
with aluminum (III) chloride in chlorobenzene at 110; for 0.5 h;Temperature;
Steps:
3.2 Example 3
(2) Add 10 g of intermediate 1 to a 250 ml reaction flask, add 100 ml of chlorobenzene, add 20.2 g of AlCl 3 , stir for 30 min, raise the temperature to 110° C., control the reaction, and after the reaction is completed, concentrate under reduced pressure, cool, and filter. Obtain 5.5g intermediate 2, yield 85%;
References:
CN107629000,2018,A Location in patent:Paragraph 0023; 0024
15450-72-3
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1127-45-3
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15450-76-7
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148-24-3
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15450-76-7
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