ChemicalBook CAS DataBase List 2-AMINO-2'-O-(2-METHOXYETHYL)ADENOSINE

2-AMINO-2'-O-(2-METHOXYETHYL)ADENOSINE synthesis

4synthesis methods

Product Name:2-AMINO-2'-O-(2-METHOXYETHYL)ADENOSINE
CAS Number:256224-13-2
Molecular formula:C13H20N6O5
Molecular Weight:340.34

16427-44-4 Synthesis

16427-44-4
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$15.00/1g

2096-10-8 Synthesis

2096-10-8
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$5.00/1g

256224-02-9 Synthesis

256224-02-9
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2-Amino-2',3'-bis-O-(2-methoxyethyl) adenosine

847647-19-2
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256224-13-2
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Yield:256224-13-2 47% ，256224-02-9 5% ，847647-19-2 25%

Reaction Conditions:

Stage #1: 2-methoxyethyl methanesulfonate;adenosine-2-aminewith sodium hydride;lithium bromide in dimethyl sulfoxide;N,N-dimethyl-formamide at 50 - 52; for 3 h;
Stage #2: 2-methoxyethyl methanesulfonatewith potassium hydroxide in dimethyl sulfoxide; for 18 h;Further stages.;

References:

Sivets, Grigorii G. [Nucleosides, nucleotides and nucleic acids,2007,vol. 26,# 10-12,p. 1237 - 1240]

6482-24-2 Synthesis