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2-Amino-3,5-dibromo-4,6-dimethylpyridine synthesis

1synthesis methods
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Yield:5407-86-3 75%

Reaction Conditions:

Stage #1: 2-Amino-4,6-dimethylpyridinewith bromine;acetic acid at 20; for 1.25 h;Inert atmosphere;
Stage #2: with sodium hydroxideInert atmosphere;Cooling with ice;

References:

Zhang, Feng;Zaidi, Saheem;Haney, Kendra M.;Kellogg, Glen E.;Zhang, Yan [Journal of Organic Chemistry,2011,vol. 76,# 19,p. 7945 - 7952] Location in patent:experimental part

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