2-BroMo-5-chloro-benzeneethanol synthesis
- Product Name:2-BroMo-5-chloro-benzeneethanol
- CAS Number:947614-94-0
- Molecular formula:C8H8BrClO
- Molecular Weight:235.51
174265-12-4
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Yield:-
Steps:
Multi-step reaction with 3 steps
1.1: potassium hexamethylsilazane / toluene / 1 h / 0 - 20 °C / Inert atmosphere
1.2: 7 h / 0 - 20 °C / Inert atmosphere
2.1: hydrogenchloride / tetrahydrofuran; water / 12 h / Reflux
3.1: sodium tetrahydroborate / methanol / 0 - 20 °C / Inert atmosphere
References:
Wurst, Jacqueline M.;Liu, Guodong;Tan, Derek S. [Journal of the American Chemical Society,2011,vol. 133,# 20,p. 7916 - 7925]
265107-67-3
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21739-93-5
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60666-70-8
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