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ChemicalBook CAS DataBase List 2-broMo-5-fluoro-1,3-diMethylbenzene

2-broMo-5-fluoro-1,3-diMethylbenzene synthesis

8synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 5 steps
1: (i) PCl5, (ii) aq. NH3
2: aq. NaOH, Br2
3: (i) aq. HCl, NaNO2, (ii) HPF6
4: H2 / Pd-C
5: (i) H2SO4, NaNO2, (ii) CuBr, aq. HBr

References:

Dewar,M.J.S.;Takeuchi,Y. [Journal of the American Chemical Society,1967,vol. 89,# 2,p. 390 - 394]

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1073338-97-2 Synthesis
2-(4-bromo-3,5-dimethylphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

1073338-97-2
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