Welcome to chemicalbook!
Chinese English Japanese Germany Korea
400-158-6606
Try our best to find the right business for you.
Do not miss inquiry messages Please log in to view all inquiry messages.

Welcome back!

ChemicalBook CAS DataBase List 2-BROMO-N-(3,5-DIMETHYL-PHENYL)-ACETAMIDE

2-BROMO-N-(3,5-DIMETHYL-PHENYL)-ACETAMIDE synthesis

2synthesis methods
10 ml freshly prepared solution of 10 % sodium  carbonate was added in a clean round bottom flask  rinsed with distilled water followed by the addition of  0.1 ml of 3,5-dimethyl aniline. Mix it properly and 1  ml of acid was added safely with the help of pipette  into the flask. Shake it well so that precipitates  appeared. Filter the ppts by using filter paper and wash the product with distilled water properly. Dry  the ppts, collect them, weigh them and save.
-

Yield:349120-86-1 97%

Reaction Conditions:

with triethylamine in dichloromethane at 0 - 20;

References:

Pitta, Eleni;Rogacki, Maciej K.;Balabon, Olga;Huss, Sophie;Cunningham, Fraser;Lopez-Roman, Eva Maria;Joossens, Jurgen;Augustyns, Koen;Ballell, Lluis;Bates, Robert H.;Van Der Veken, Pieter [Journal of Medicinal Chemistry,2016,vol. 59,# 14,p. 6709 - 6728]

2-BROMO-N-(3,5-DIMETHYL-PHENYL)-ACETAMIDE Related Search: