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2-bromo-N-methylpyridin-3-amine synthesis

3synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 2 steps
1: sodium hydride / N,N-dimethyl-formamide / 1.5 h / 0 - 5 °C
2: trifluoroacetic acid / dichloromethane / 2 h / 0 - 25 °C

References:

Lach, Franck;Koza, Patrice [ACS Combinatorial Science,2012,vol. 14,# 9,p. 491 - 495]