ChemicalBook CAS DataBase List 2-CHLORO-N-(2,3-DIMETHYL-PHENYL)-ACETAMIDE

2-CHLORO-N-(2,3-DIMETHYL-PHENYL)-ACETAMIDE synthesis

3synthesis methods

Product Name:2-CHLORO-N-(2,3-DIMETHYL-PHENYL)-ACETAMIDE
CAS Number:2564-07-0
Molecular formula:C10H12ClNO
Molecular Weight:197.66

79-04-9 Synthesis

79-04-9
354 suppliers
$12.00/5g

87-59-2 Synthesis

87-59-2
284 suppliers
$13.00/1g

2-CHLORO-N-(2,3-DIMETHYL-PHENYL)-ACETAMIDE

2564-07-0
70 suppliers
$28.60/50MG

Yield:2564-07-0 96%

Reaction Conditions:

with sodium hydroxide in dichloromethane;water; for 18 h;

Steps:

17A EXAMPLE 17 ; 2-[4-(3-cyano-2-pyridinyl)-1-piperazinyl]-N-(2.3-dimethylphenyl)acetamide ; EXAMPLE 17A ; 2-chloro-N-(2,3-dimethylphenyl)acetamide

The procedure described in Example 16A was followed, substituting 2,3-dimethylaniline for 3,5-dimethylaniline to provide the title compound (96% yield) as a white solid. 1H NMR (300 MHz, DMSO-d6) ? 2.07 (s, 3H), 2.24 (s, 3H), 4.28 (s, 2H), 7.07 (m, 3H), 9.70 (br s, 1H); MS (DCI/NH3) m/e 198 (M+H)+.

References:

US2003/232836,2003,A1 Location in patent:Page 44

87-59-2 Synthesis

87-59-2
284 suppliers
$13.00/1g

2564-07-0
70 suppliers
$28.60/50MG

References

95-64-7
228 suppliers
$5.00/5G

79-04-9 Synthesis

79-04-9
354 suppliers
$12.00/5g

2564-07-0
70 suppliers
$28.60/50MG

References

2-CHLORO-N-(2,3-DIMETHYL-PHENYL)-ACETAMIDE Related Search:

1-BENZYL-N,4-DIMETHYLPIPERIDIN-3-AMINE DIHYDROCHLORIDE N-methyl-N-((3R,4R)-4-methylpiperidin-3-yl)-7H-pyrrolo[2,3-d]pyrimidin-4-amine 7H-Pyrrolo[2,3-d]pyriMidin-4-aMine, N-Methyl-N-[(3R,4R)-4-Methyl-1-(phenylMethyl)-3-piperidinyl]-7-[(4-Met hylphenyl)sulfonyl]- Tofacitinib citrate