2-cyclopropoxyacetic acid synthesis
- Product Name:2-cyclopropoxyacetic acid
- CAS Number:246869-07-8
- Molecular formula:C5H8O3
- Molecular Weight:116.12
16545-68-9
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79-08-3
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Yield:246869-07-8 100%
Reaction Conditions:
Stage #1: cyclopropyl alcoholwith sodium hydride in tetrahydrofuran at 0; for 2 h;Inert atmosphere;
Stage #2: 2-bromoacetic acid in tetrahydrofuran at 0 - 20; for 20 h;Inert atmosphere;
References:
Meng, Wei;Pi, Zulan;Brigance, Robert;Rossi, Karen A.;Schumacher, William A.;Bostwick, Jeffrey S.;Gargalovic, Peter S.;Onorato, Joelle M.;Luk, Chiuwa E.;Generaux, Claudia N.;Wang, Tao;Wexler, Ruth R.;Finlay, Heather J. [Journal of Medicinal Chemistry,2021,vol. 64,# 24,p. 18102 - 18113] Location in patent:supporting information
16545-68-9
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3926-62-3
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246869-07-8
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