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ChemicalBook CAS DataBase List 2'-Deoxycytidine hydrochloride

2'-Deoxycytidine hydrochloride synthesis

1synthesis methods
-

Yield: 78%

Reaction Conditions:

Stage #1:p-toluenesulfonyl chloride;3',5'-O-bis(4-chlorobenzoyl)-2'-deoxy-β-D-cytidine with sodium hydroxide in methanol at 40; for 4.5 h;Large scale;
Stage #2: with hydrogenchloride in methanolLarge scale;

References:

Komatsu, Hironori;Morizane, Kunihiko;Kohno, Toshiyuki;Tanikawa, Hiroharu [Organic Process Research and Development,2004,vol. 8,# 4,p. 564 - 567]

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