ChemicalBook CAS DataBase List 2-(Dicyclohexylphosphino)-2'-methoxybiphenyl

2-(Dicyclohexylphosphino)-2'-methoxybiphenyl synthesis

1synthesis methods

Product Name:2-(Dicyclohexylphosphino)-2'-methoxybiphenyl
CAS Number:255835-82-6
Molecular formula:C25H33OP
Molecular Weight:380.5

694-80-4 Synthesis

694-80-4
388 suppliers
$5.00/10g

16750-63-3
64 suppliers
$66.09/100ml

16523-54-9 Synthesis

16523-54-9
257 suppliers
$8.00/1g

2-(Dicyclohexylphosphino)-2'-methoxybiphenyl

255835-82-6
101 suppliers
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Yield: 48%

Reaction Conditions:

Stage #1:2-bromo-1-chlorobenzene;2-methoxyphenylmagnesium bromide with magnesium in tetrahydrofuran at 60; for 2.5 h;
Stage #2:chlorodicyclohexylphosphane with copper(l) chloride in tetrahydrofuran at 20; for 16 h;Further stages.;

References:

Parrish;Buchwald [Journal of Organic Chemistry,2001,vol. 66,# 11,p. 3820 - 3827]

2-(Dicyclohexylphosphino)-2'-methoxybiphenyl Related Search:

2-(Diphenylphosphino)-2'-methylbiphenyl 2-Dicyclohexylphosphino-2',6'-bis(diMethylaMino)-1,1'-biphenyl, Min. 98% Cphos X-PHOS 2-DI-TERT-BUTYLPHOSPHINO-2',4',6'-TRIISOPROPYLBIPHENYL 2-Dicyclohexylphosphino-2'-(N,N-dimethylamino)biphenyl 2-(Dicyclohexylphosphino)biphenyl 2-Dicyclohexylphosphino-2',6'-dimethoxybiphenyl 2-(Dicyclohexylphosphino)-2'-methylbiphenyl 2-DICYCLOHEXYLPHOSPHINO-2',6'-DIISOPROPOXYBIPHENYL