![](/CAS/GIF/4536-30-5.gif)
2-(DODECYLOXY)ETHANOL synthesis
- Product Name:2-(DODECYLOXY)ETHANOL
- CAS Number:4536-30-5
- Molecular formula:C14H30O2
- Molecular Weight:230.39
![Ethylene glycol](/CAS/GIF/107-21-1.gif)
107-21-1
1314 suppliers
$10.00/25g
![1-Bromododecane](/CAS/GIF/143-15-7.gif)
143-15-7
431 suppliers
$5.00/25g
![2-(DODECYLOXY)ETHANOL](/CAS/GIF/4536-30-5.gif)
4536-30-5
50 suppliers
$186.00/1ml
Yield:4536-30-5 69%
Reaction Conditions:
with tetrabutylammomium bromide;potassium hydroxide in 1,4-dioxane at 100 - 105;
Steps:
Ethylene glycol and diethylene glycol monoalkyl ethers 8a-e (general procedure).
General procedure: Dioxane (15 mL), alkyl halide (25 mmol), and tetrabutylammonium bromide (0.4 g, 1.2 mmol) were added to a solution of KOH (1.6 g, 27.5 mmol) in glycol (75-125 mmol). After stirring at 100-105 °C for 5-10 h, the reaction mixture was diluted with CHCl3 (15 mL) and water (10 mL). The organic layer was separated, washed with water (3×20 mL), dried with Na2SO4, and evaporated in vacuo, and the residue was distilled using Vigreux column. For each particular case, the ratio of the starting reagents, yields, physicochemical parameters, and 1H NMR spectral data for monoalkyl ethers 8a-e are givenin Table 6.
References:
Kharlamov;Artyushin;Bondarenko [Russian Chemical Bulletin,2014,vol. 63,# 11,p. 2445 - 2454][Izv. Akad. Nauk, Ser. Khim.,2014,# 11,p. 2445 - 2454]
![1-Iodododecane](/CAS/GIF/4292-19-7.gif)
4292-19-7
145 suppliers
$18.00/1g
![Ethylene glycol](/CAS/GIF/107-21-1.gif)
107-21-1
1314 suppliers
$10.00/25g
![2-(DODECYLOXY)ETHANOL](/CAS/GIF/4536-30-5.gif)
4536-30-5
50 suppliers
$186.00/1ml
![Ethylene carbonate](/CAS/GIF/96-49-1.gif)
96-49-1
484 suppliers
$6.00/100g
![1-Dodecanol](/CAS/GIF/112-53-8.gif)
112-53-8
422 suppliers
$10.00/5g
![2-(DODECYLOXY)ETHANOL](/CAS/GIF/4536-30-5.gif)
4536-30-5
50 suppliers
$186.00/1ml
![1-DODECENE](/CAS/GIF/112-41-4.gif)
112-41-4
216 suppliers
$8.00/10g
![Ethylene glycol](/CAS/GIF/107-21-1.gif)
107-21-1
1314 suppliers
$10.00/25g
![2-(DODECYLOXY)ETHANOL](/CAS/GIF/4536-30-5.gif)
4536-30-5
50 suppliers
$186.00/1ml
![1-DODECENE](/CAS/GIF/112-41-4.gif)
112-41-4
216 suppliers
$8.00/10g
![Ethylene glycol](/CAS/GIF/107-21-1.gif)
107-21-1
1314 suppliers
$10.00/25g
![2-(DODECYLOXY)ETHANOL](/CAS/GIF/4536-30-5.gif)
4536-30-5
50 suppliers
$186.00/1ml
![1,2-DIDODECYLOXYETHANE](/CAS/20180629/GIF/22870-18-4.gif)
22870-18-4
3 suppliers
$57.00/250mg