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2-(ethenesulfonyl)pyridine synthesis

3synthesis methods
-

Yield:349491-22-1 86%

Reaction Conditions:

Stage #1: 2,2'-dipyridyldisulphide;vinyl magnesium bromide in tetrahydrofuran;cooling;
Stage #2: with Na2W7O4*2H2O;dihydrogen peroxide in water;ethyl acetate;cooling;

References:

Llamas, Tomas;Arrayas, Ramon Gomez;Carretero, Juan C. [Organic Letters,2006,vol. 8,# 9,p. 1795 - 1798]