2-Ethyl-1-methylpyrrolidine synthesis
- Product Name:2-Ethyl-1-methylpyrrolidine
- CAS Number:26158-82-7
- Molecular formula:C7H15N
- Molecular Weight:113.2
Yield:26158-82-7 0.4 mol
Reaction Conditions:
in diethyl ether at 60; for 24 h;Inert atmosphere;Sealed tube;
Steps:
4
Ethyl pyrrolidine (5.00 mol) obtained above was put in a pressure-resistant container made of PFA together with 200 mL of dry diethyl ether and 0.500 mol of iodomethyl under argon atmosphere and sealed, and then reacted at 60 ° C. for 24 hours .The solution after the reaction was distilled under reduced pressure to obtain 0.400 mol of 2-ethyl-1-methylpyrrolidine
References:
JP2017/178792,2017,A Location in patent:Paragraph 0062
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