![](/CAS/GIF/149-57-5.gif)
2-Ethylhexanoic acid synthesis
- Product Name:2-Ethylhexanoic acid
- CAS Number:149-57-5
- Molecular formula:C8H16O2
- Molecular Weight:144.21
![2-Ethylhexanoic acid 2-Ethylhexanoic acid](/NewsImg/2023-12-18/6383849270228070202586132.jpg)
![2-ETHYLHEXANAL](/CAS/GIF/123-05-7.gif)
123-05-7
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$10.00/5mL
![2-Ethylhexanoic acid](/CAS/GIF/149-57-5.gif)
149-57-5
517 suppliers
$5.00/25g
Yield:149-57-5 99.1%
Reaction Conditions:
with C43H56IO4P;anhydrous potassium acetate;Cs2CO3 at 35; for 6 h;Cooling;Reagent/catalyst;
Steps:
6-12 Example 7
In a dry 1L three-neck bottle, Add isooctyl aldehyde (80g, 0.62mol) And the solvent 2-ethylhexanoic acid (240g, 1.66mol), ligand L8 (5.24mg, 0.007mmol), cesium carbonate (18.24mg, 0.056mmol), potassium acetate 160mg, placed in a water bath, mechanical under nitrogen atmosphere Stir, after the temperature rises to 30 ° C, Air flow was started at a flow rate of 11.9 g/h, and the reaction temperature was maintained at 30-35 ° C by adding cooling water to the water bath. After 6 hours of reaction, the conversion of isooctyl aldehyde was calculated to be 99.6%. The selectivity of 2-ethylhexanoic acid was 99.5%, and the yield was 99.10%.
References:
CN109134538,2019,A Location in patent:Paragraph 0091-0104
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589-82-2
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![2-Ethylhexanol](/CAS/GIF/104-76-7.gif)
104-76-7
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![2-Ethylhexanoic acid](/CAS/GIF/149-57-5.gif)
149-57-5
517 suppliers
$5.00/25g