2-Hexyne, 6-chloro- synthesis
- Product Name:2-Hexyne, 6-chloro-
- CAS Number:28077-73-8
- Molecular formula:C6H9Cl
- Molecular Weight:116.59
Yield: 72%
Reaction Conditions:
Stage #1:1-chloro-4-pentyne with n-butyllithium in tetrahydrofuran;hexane at -78; for 1 h;
Stage #2:methyl iodide in tetrahydrofuran;hexane at 20; for 1 h;
References:
Zelenay, Benjamin;Munton, Peter;Tian, Xiaojie;Díez-González, Silvia [European Journal of Organic Chemistry,2019,vol. 2019,# 29,p. 4725 - 4730] Location in patent:supporting information
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