2-IODOBENZOYLACETONITRILE synthesis
2synthesis methods
- Product Name:2-IODOBENZOYLACETONITRILE
- CAS Number:158387-19-0
- Molecular formula:C9H6INO
- Molecular Weight:271.05
Yield:158387-19-0 79%
Reaction Conditions:
with sodium hydride in tetrahydrofuran;mineral oil; for 2 h;Reflux;
References:
Boelke, Andreas;Caspers, Lucien D.;Kuczmera, Thomas J.;Lork, Enno;Nachtsheim, Boris J. [Organic Letters,2020,vol. 22,# 18,p. 7261 - 7266] Location in patent:supporting information