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2-METHOXY-4,6-DIMETHYLBENZALDEHYDE synthesis

7synthesis methods
-

Yield:19447-00-8 10% ,51926-66-0 89%

Reaction Conditions:

with titanium tetrachloride in dichloromethane;1.) -78 deg C, 30 min, 2.) -78 deg C to 0 deg C, 1 h, 3.) 0 deg C, 15 min;

References:

Kraus, George A.;Zhao, Guohua [Journal of Organic Chemistry,1996,vol. 61,# 8,p. 2770 - 2773]