![](/CAS/GIF/1120-72-5.gif)
2-Methylcyclopentanone synthesis
- Product Name:2-Methylcyclopentanone
- CAS Number:1120-72-5
- Molecular formula:C6H10O
- Molecular Weight:98.14
![methyl 1-methyl-2-oxocyclopentanecarboxylate](/CAS/GIF/30680-84-3.gif)
30680-84-3
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$106.00/5MG
![2-Methylcyclopentanone](/CAS/GIF/1120-72-5.gif)
1120-72-5
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$8.00/1g
Yield:1120-72-5 95%
Reaction Conditions:
with sulfuric acid in water at 100; for 10 h;
Steps:
2 Preparation of 2-methylcyclopentanone
Methyl 1-methyl-2-oxocyclopentanecarboxylate (200 g, 1.3 mol), water (1.5 L), concentrated sulfuric acid (7.5 mL, 0.13 mol),After the addition, the temperature was raised to 100 ° C for 10 hours.The system is cooled to room temperature,The organic phase was combined and washed with 5% sodium hydrogencarbonate and saturated brine.Drying over anhydrous sodium sulfate, distilling off the solvent and distilling under reduced pressure to give 2-methylcyclopentanone 120 g.The yield was 95%.
References:
CN110204500,2019,A Location in patent:Paragraph 0055-0057
![2-METHYLCYCLOPENTANOL](/CAS/GIF/24070-77-7.gif)
24070-77-7
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1120-72-5
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$8.00/1g
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1192-62-7
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![2-Methylcyclopentanone](/CAS/GIF/1120-72-5.gif)
1120-72-5
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$8.00/1g
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329971-02-0
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![2-Methylcyclopentanone](/CAS/GIF/1120-72-5.gif)
1120-72-5
143 suppliers
$8.00/1g