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2-VALERYLPYRIDINE synthesis

8synthesis methods
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Yield:7137-97-5 85%

Reaction Conditions:

Stage #1: 1-bromo-butanewith iodine;magnesium in tetrahydrofuran;
Stage #2: 2-Cyanopyridine in tetrahydrofuran at 0;

References:

Yang, Hailong;Huo, Ningning;Yang, Ping;Pei, Hao;Lv, Hui;Zhang, Xumu [Organic Letters,2015,vol. 17,# 17,p. 4144 - 4147] Location in patent:supporting information

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