![](/CAS/20180906/GIF/208111-36-8.gif)
N-(3-Chloro-4-fluorobenzoyl)-4-fluoro-4-N-(3-Chloro-4-fluorobenzoyl)-4-fluoro-4-hydroxymethylpiperidine synthesis
- Product Name:N-(3-Chloro-4-fluorobenzoyl)-4-fluoro-4-N-(3-Chloro-4-fluorobenzoyl)-4-fluoro-4-hydroxymethylpiperidine
- CAS Number:208111-36-8
- Molecular formula:C13H14ClF2NO2
- Molecular Weight:289.71
![(3-Chloro-4-fluoro-phenyl)-(1-oxa-6-aza-spiro[2.5]oct-6-YL)-methanone](/CAS/20210305/GIF/208111-51-7.gif)
208111-51-7
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![N-(3-Chloro-4-fluorobenzoyl)-4-fluoro-4-N-(3-Chloro-4-fluorobenzoyl)-4-fluoro-4-hydroxymethylpiperidine](/CAS/20180906/GIF/208111-36-8.gif)
208111-36-8
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Yield:208111-36-8 50%
Reaction Conditions:
with pyridine hydrogenfluoride in dichloromethane;a) -10 deg C, 15 min, b) RT, 16 h;
References:
Vacher, Bernard;Bonnaud, Bernard;Funes, Philippe;Jubault, Nathalie;Koek, Wouter;Assié, Marie-Bernadette;Cosi, Cristina;Kleven, Mark [Journal of Medicinal Chemistry,1999,vol. 42,# 9,p. 1648 - 1660]
![3-Chloro-4-fluorobenzoyl chloride](/CAS/GIF/65055-17-6.gif)
65055-17-6
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![N-(3-chloro-4-fluorobenzoyl)-piperidine-4-one](/CAS/20180601/GIF/223632-64-2.gif)
223632-64-2
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208111-36-8
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