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ChemicalBook CAS DataBase List 3-(2,6-DICHLOROPHENYL)-5-METHYL-4-ISOXAZOLECARBONITRILE

3-(2,6-DICHLOROPHENYL)-5-METHYL-4-ISOXAZOLECARBONITRILE synthesis

1synthesis methods
-

Yield:21486-28-2 10%

Reaction Conditions:

Stage #1: but-2-enenitrile;2,6-dichlorobenzohydroximoyl chloridewith triethylamine in tetrahydrofuran at 20 - 67; for 4 h;
Stage #2: with nickel(IV) oxide in benzene;Heating;Further stages.;

References:

Easton;Heath;Hughes;Lee;Savage;Simpson;Tiekink;Vuckovic;Webster [Journal of the Chemical Society. Perkin Transactions 1 (2001),2001,# 10,p. 1168 - 1174]