1H-Pyrrolo[3,2-c]pyridine,2,3-dihydro-1-methyl-(9CI) synthesis

6synthesis methods

Product Name:1H-Pyrrolo[3,2-c]pyridine,2,3-dihydro-1-methyl-(9CI)
CAS Number:219834-79-4
Molecular formula:C8H10N2
Molecular Weight:134.18

98400-69-2 Synthesis

98400-69-2
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$6.00/1g

1H-Pyrrolo[3,2-c]pyridine,2,3-dihydro-1-methyl-(9CI)

219834-79-4
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Yield:-

Steps:

Multi-step reaction with 3 steps
1.1: t-butyllithium / tetrahydrofuran; pentane / 3.5 h / -78 - -15 °C
1.2: 75 percent / tetrahydrofuran; pentane / 2 h / -78 - 20 °C
2.1: 100 percent / triethylamine; methanesulfonyl chloride / CH₂Cl₂ / 2 h / -10 - 20 °C
3.1: 11.0 g / diisobutylaluminum hydride / CH₂Cl₂ / 20 h / Heating

References:

Spivey, Alan C.;Fekner, Tomasz;Spey, Sharon E.;Adams, Harry [Journal of Organic Chemistry,1999,vol. 64,# 26,p. 9430 - 9443]

257937-14-7
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219834-79-4
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References

1H-Pyrrolo[3,2-c]pyridine-1-carboxylic acid,2,3-dihydro-1,1-diemthylethyl ester

219834-81-8
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219834-79-4
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References

219834-80-7 Synthesis

219834-80-7
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$165.19/100mg

219834-79-4
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1H-Pyrrolo[3,2-c]pyridine,2,3-dihydro-(8CI,9CI)

23596-28-3
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$65.00/10mg

219834-79-4
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References