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Phospholane, 1-hydroxy-2,5-diphenyl-, 1-oxide, (2R,5R)- synthesis
- Product Name:Phospholane, 1-hydroxy-2,5-diphenyl-, 1-oxide, (2R,5R)-
- CAS Number:226393-33-5
- Molecular formula:C16H17O2P
- Molecular Weight:272.28
Yield:81 % ee
Reaction Conditions:
with hydrogenchloride;water in methanol at 60; for 16 h;Overall yield = 75 %; Overall yield = 0.225 g;
References:
Hintermann, Lukas;Schmitz, Marco;Maltsev, Olegv.;Naumov, Pance [Synthesis,2013,vol. 45,# 3,art. no. SS-2012-T0745-FA,p. 308 - 325] Location in patent:supporting information
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