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Benzenesulfonic acid, 4-methyl-, methylazanyl ester synthesis
- Product Name:Benzenesulfonic acid, 4-methyl-, methylazanyl ester
- CAS Number:25370-97-2
- Molecular formula:C8H11NO3S
- Molecular Weight:201.24
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98-59-9
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Yield:-
Steps:
Multi-step reaction with 2 steps
1.1: potassium carbonate / tetrahydrofuran; water / 5 h / 0 - 20 °C / Inert atmosphere; Cooling with ice
1.2: 18 h / 20 °C / Inert atmosphere
2.1: trifluoroacetic acid / dichloromethane / 3 h / 0 °C / Inert atmosphere
References:
Paudyal, Mahesh P.;Wang, Mingliang;Siitonen, Juha H.;Hu, Yimin;Yousufuddin, Muhammed;Shen, Hong C.;Falck, John R.;Kürti, László [Organic and Biomolecular Chemistry,2021,vol. 19,# 3,p. 557 - 560]
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25370-96-1
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![Benzenesulfonic acid, 4-methyl-, methylazanyl ester](/CAS/20210111/GIF/25370-97-2.gif)
25370-97-2
5 suppliers
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