3-[1-(4-METHOXY-PHENYL)-2-NITRO-ETHYL]-1H-INDOLE synthesis
- Product Name:3-[1-(4-METHOXY-PHENYL)-2-NITRO-ETHYL]-1H-INDOLE
- CAS Number:33723-33-0
- Molecular formula:C17H16N2O3
- Molecular Weight:296.32
Yield:33723-33-0 99%
Reaction Conditions:
Stage #1: 4-methoxy-β-nitrostyrenewith (S)-10,10'-bis[(S)-4-isopropyl-4,5-dihydrooxazol-2-yl]-9,9'-biphenanthrene;zinc(II) trifluoroacetate in diethyl ether at 20; for 0.25 h;Inert atmosphere;
Stage #2: indole in diethyl ether at 20;Inert atmosphere;Friedel-Crafts alkylation;
References:
Lin, Shuang-zheng;You, Tian-pa [Tetrahedron,2009,vol. 65,# 5,p. 1010 - 1016] Location in patent:experimental part
123-11-5
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