![](/CAS/GIF/31995-08-1.gif)
3-(2-Methoxyethoxy)prop-1-yne synthesis
- Product Name:3-(2-Methoxyethoxy)prop-1-yne
- CAS Number:31995-08-1
- Molecular formula:C6H10O2
- Molecular Weight:114.14
![2-Methoxyethanol](/CAS/GIF/109-86-4.gif)
109-86-4
521 suppliers
$11.00/25g
![propargyl bromide](/CAS/GIF/106-96-7.gif)
106-96-7
332 suppliers
$31.00/25g
![3-(2-Methoxyethoxy)prop-1-yne](/CAS/GIF/31995-08-1.gif)
31995-08-1
26 suppliers
$114.00/1g
Yield:31995-08-1 79%
Reaction Conditions:
Stage #1: 2-methoxy-ethanolwith sodium hydride in tetrahydrofuran;mineral oil at 0; for 1 h;Inert atmosphere;Williamson synthesis;
Stage #2: propargyl bromide in tetrahydrofuran;mineral oil at 0; for 4 h;Inert atmosphere;Williamson synthesis;
References:
Nanashima, Yutaka;Shibata, Rena;Miyakoshi, Ryo;Yokoyama, Akihiro;Yokozawa, Tsutomu [Journal of Polymer Science, Part A: Polymer Chemistry,2012,vol. 50,# 17,p. 3628 - 3640] Location in patent:experimental part
![2-Methoxyethanol](/CAS/GIF/109-86-4.gif)
109-86-4
521 suppliers
$11.00/25g
![3-Chloropropyne](/CAS/GIF/624-65-7.gif)
624-65-7
366 suppliers
$25.00/5mL
![3-(2-Methoxyethoxy)prop-1-yne](/CAS/GIF/31995-08-1.gif)
31995-08-1
26 suppliers
$114.00/1g