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(3β,20S)-20-Formyl-3-hydroxy-5-pregnene synthesis

7synthesis methods
10211-88-8 Synthesis
(3β,20S)-20-Formyl-3-hydroxy-5-pregnene 3-O-Acetate

10211-88-8
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(3β,20S)-20-Formyl-3-hydroxy-5-pregnene

53906-49-3
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Yield:53906-49-3 90%

Reaction Conditions:

with water;potassium carbonate in methanol;Inert atmosphere;

References:

Gigante, Federica;Kaiser, Marcel;Brun, Reto;Gilbert, Ian H. [Bioorganic and Medicinal Chemistry,2009,vol. 17,# 16,p. 5950 - 5961] Location in patent:experimental part