![](/CAS/GIF/13636-88-9.gif)
3,3-BIS-METHYLSULFANYL-1-PHENYL-PROPENONE synthesis
- Product Name:3,3-BIS-METHYLSULFANYL-1-PHENYL-PROPENONE
- CAS Number:13636-88-9
- Molecular formula:C11H12OS2
- Molecular Weight:224.34
![Carbon disulfide](/CAS/GIF/75-15-0.gif)
75-15-0
235 suppliers
$40.00/100g
![Acetophenone](/CAS/GIF/98-86-2.gif)
98-86-2
743 suppliers
$9.00/5g
![Iodomethane](/CAS/GIF/74-88-4.gif)
74-88-4
342 suppliers
$15.00/10g
![3,3-BIS-METHYLSULFANYL-1-PHENYL-PROPENONE](/CAS/GIF/13636-88-9.gif)
13636-88-9
24 suppliers
$106.00/50MG
Yield:13636-88-9 87%
Reaction Conditions:
Stage #1: carbon disulfide;acetophenonewith sodium tertiary butoxide in toluene at 0; for 5 h;Inert atmosphere;
Stage #2: iodomethane in methanol;toluene; for 0.25 h;Reflux;
References:
Smyth, Lynette A.;Matthews, Thomas P.;Horton, Peter N.;Hursthouse, Michael B.;Collins, Ian [Tetrahedron,2010,vol. 66,# 15,p. 2843 - 2854] Location in patent:experimental part
![Carbon disulfide](/CAS/GIF/75-15-0.gif)
75-15-0
235 suppliers
$40.00/100g
![Methyl bromide](/CAS/GIF/74-83-9.gif)
74-83-9
2 suppliers
$28.30/1ML
![Acetophenone](/CAS/GIF/98-86-2.gif)
98-86-2
743 suppliers
$9.00/5g
![3,3-BIS-METHYLSULFANYL-1-PHENYL-PROPENONE](/CAS/GIF/13636-88-9.gif)
13636-88-9
24 suppliers
$106.00/50MG
![Acetophenone](/CAS/GIF/98-86-2.gif)
98-86-2
743 suppliers
$9.00/5g
![Iodomethane](/CAS/GIF/74-88-4.gif)
74-88-4
342 suppliers
$15.00/10g
![3,3-BIS-METHYLSULFANYL-1-PHENYL-PROPENONE](/CAS/GIF/13636-88-9.gif)
13636-88-9
24 suppliers
$106.00/50MG
![Methanol](/CAS/GIF/67-56-1.gif)
67-56-1
739 suppliers
$9.00/25ml
![Benzenepropane(dithioic) acid, β-oxo-, methyl ester](/CAS/20210305/GIF/20365-21-3.gif)
20365-21-3
0 suppliers
inquiry
![3,3-BIS-METHYLSULFANYL-1-PHENYL-PROPENONE](/CAS/GIF/13636-88-9.gif)
13636-88-9
24 suppliers
$106.00/50MG
![2-[bis(methylsulfanyl)methylidene]-1-phenylbutane-1,3-dione](/CAS/20180529/GIF/29866-41-9.gif)
29866-41-9
1 suppliers
inquiry
![3,3-BIS-METHYLSULFANYL-1-PHENYL-PROPENONE](/CAS/GIF/13636-88-9.gif)
13636-88-9
24 suppliers
$106.00/50MG