3-(3-METHYLPHENYL)BENZALDEHYDE synthesis
- Product Name:3-(3-METHYLPHENYL)BENZALDEHYDE
- CAS Number:216443-78-6
- Molecular formula:C14H12O
- Molecular Weight:196.24
108-41-8
257 suppliers
$19.00/10g
587-04-2
413 suppliers
$7.00/25g
216443-78-6
57 suppliers
$45.00/250mg
Yield:216443-78-6 71%
Reaction Conditions:
Stage #1: 1-chloro-3-methylbenzenewith tetrahydroxydiboron;ethanol;XPhos-Pd-G2;potassium acetate;XPhos in water at 80; for 15 h;Inert atmosphere;Miyaura Borylation Reaction;
Stage #2: m-Chlorobenzaldehydewith potassium carbonate in water at 80; for 15 h;Inert atmosphere;Suzuki Coupling;
References:
Molander, Gary A.;Trice, Sarah L. J.;Kennedy, Steven M. [Journal of Organic Chemistry,2012,vol. 77,# 19,p. 8678 - 8688]
3132-99-8
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$5.00/10g
17933-03-8
360 suppliers
$5.00/1g
216443-78-6
57 suppliers
$45.00/250mg