ChemicalBook CAS DataBase List 3-(4-BROMOPHENYL)-2-CHLOROQUINOLINE

3-(4-BROMOPHENYL)-2-CHLOROQUINOLINE synthesis

1synthesis methods

Product Name:3-(4-BROMOPHENYL)-2-CHLOROQUINOLINE
CAS Number:85274-82-4
Molecular formula:C15H9BrClN
Molecular Weight:318.6

Formamide, N-[2-[2-(4-bromophenyl)ethynyl]phenyl]-

1200688-13-6
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85274-82-4
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$265.00/250mg

Yield:85274-82-4 99%

Reaction Conditions:

Stage #1: C₁₅H₁₀BrNOwith N-ethyl-N,N-diisopropylamine;trichlorophosphate in dichloromethane at 0;Inert atmosphere;
Stage #2: with tetrabutyl-ammonium chloride in dichloromethane at 40; for 15 h;Inert atmosphere;

References:

Liu, Lanying;Wang, Yong;Wang, Honggen;Peng, Changlan;Zhao, Jiaji;Zhu, Qiang [Tetrahedron Letters,2009,vol. 50,# 48,p. 6715 - 6719] Location in patent:experimental part

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