3-(4-HYDROXY-PHENYL)-3-OXO-PROPIONITRILE synthesis

Yield:70591-87-6 41%

Reaction Conditions:

with tris(6,6'-diamino-2,2'-bipyridine);4,4-diphenyl-1,3,5,7,8-pentamethyl-2,6-diethyl-4-bora-3a,4a-diaza-s-indacene;Br₂Ni*3H₂O;water;N-ethyl-N,N-diisopropylamine in N,N-dimethyl-formamide;acetonitrile at 20; for 24 h;Glovebox;Irradiation;Inert atmosphere;

References:

Yang, Liu;Huang, Zhiyan;Li, Gang;Zhang, Wei;Cao, Rui;Wang, Chao;Xiao, Jianliang;Xue, Dong [Angewandte Chemie - International Edition,2018,vol. 57,# 7,p. 1968 - 1972][Angew. Chem.,2018,vol. 130,p. 1986 - 1990,5] Location in patent:supporting information