3-(4-HYDROXY-PHENYL)-3-OXO-PROPIONITRILE synthesis
- Product Name:3-(4-HYDROXY-PHENYL)-3-OXO-PROPIONITRILE
- CAS Number:70591-87-6
- Molecular formula:C9H7NO2
- Molecular Weight:161.16
4640-66-8
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Yield:70591-87-6 41%
Reaction Conditions:
with tris(6,6'-diamino-2,2'-bipyridine);4,4-diphenyl-1,3,5,7,8-pentamethyl-2,6-diethyl-4-bora-3a,4a-diaza-s-indacene;Br2Ni*3H2O;water;N-ethyl-N,N-diisopropylamine in N,N-dimethyl-formamide;acetonitrile at 20; for 24 h;Glovebox;Irradiation;Inert atmosphere;
References:
Yang, Liu;Huang, Zhiyan;Li, Gang;Zhang, Wei;Cao, Rui;Wang, Chao;Xiao, Jianliang;Xue, Dong [Angewandte Chemie - International Edition,2018,vol. 57,# 7,p. 1968 - 1972][Angew. Chem.,2018,vol. 130,p. 1986 - 1990,5] Location in patent:supporting information
99-93-4
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