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70591-87-6

3-(4-HYDROXY-PHENYL)-3-OXO-PROPIONITRILE synthesis

4synthesis methods
4640-66-8 Synthesis
4-CHLOROBENZOYLACETONITRILE

4640-66-8
249 suppliers
$6.00/1g

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Yield:70591-87-6 41%

Reaction Conditions:

with tris(6,6'-diamino-2,2'-bipyridine);4,4-diphenyl-1,3,5,7,8-pentamethyl-2,6-diethyl-4-bora-3a,4a-diaza-s-indacene;Br2Ni*3H2O;water;N-ethyl-N,N-diisopropylamine in N,N-dimethyl-formamide;acetonitrile at 20; for 24 h;Glovebox;Irradiation;Inert atmosphere;

References:

Yang, Liu;Huang, Zhiyan;Li, Gang;Zhang, Wei;Cao, Rui;Wang, Chao;Xiao, Jianliang;Xue, Dong [Angewandte Chemie - International Edition,2018,vol. 57,# 7,p. 1968 - 1972][Angew. Chem.,2018,vol. 130,p. 1986 - 1990,5] Location in patent:supporting information

773837-37-9 Synthesis
sodium:cyanide

773837-37-9
0 suppliers
inquiry

2491-38-5 Synthesis
2-Bromo-4'-hydroxyacetophenone

2491-38-5
260 suppliers
$5.00/100mg

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