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ChemicalBook CAS DataBase List 3,4-DIMETHOXYBENZOYLACETONITRILE

3,4-DIMETHOXYBENZOYLACETONITRILE synthesis

7synthesis methods
-

Yield:4640-69-1 100%

Reaction Conditions:

Stage #1: acetonitrilewith n-butyllithium in tetrahydrofuran;hexane at -78; for 1 h;
Stage #2: methyl 3,4-dimethoxybenzoate in tetrahydrofuran;hexane at -78 - -45;Further stages.;

References:

Fang, Zhenglai;Song, Yunlong;Sarkar, Taradas;Hamel, Ernest;Fogler, William E.;Agoston, Gregory E.;Fanwick, Phillip E.;Cushman, Mark [Journal of Organic Chemistry,2008,vol. 73,# 11,p. 4241 - 4244]

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