![](/CAS/GIF/4640-69-1.gif)
3,4-DIMETHOXYBENZOYLACETONITRILE synthesis
- Product Name:3,4-DIMETHOXYBENZOYLACETONITRILE
- CAS Number:4640-69-1
- Molecular formula:C11H11NO3
- Molecular Weight:205.21
Yield:4640-69-1 100%
Reaction Conditions:
Stage #1: acetonitrilewith n-butyllithium in tetrahydrofuran;hexane at -78; for 1 h;
Stage #2: methyl 3,4-dimethoxybenzoate in tetrahydrofuran;hexane at -78 - -45;Further stages.;
References:
Fang, Zhenglai;Song, Yunlong;Sarkar, Taradas;Hamel, Ernest;Fogler, William E.;Agoston, Gregory E.;Fanwick, Phillip E.;Cushman, Mark [Journal of Organic Chemistry,2008,vol. 73,# 11,p. 4241 - 4244]
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