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872492-59-6

(3-BroMo-5-Methyl-pyridin-2-yl)-Methyl-aMine synthesis

1synthesis methods
-

Yield:872492-59-6 87%

Reaction Conditions:

Stage #1: 2-Amino-3-bromo-5-methylpyridinewith sodium hydride in tetrahydrofuran at 0 - 20;
Stage #2: iodomethane in tetrahydrofuran at 20; for 4 h;

References:

Abbiati, Giorgio;Beccalli, Egle M.;Broggini, Gianluigi;Paladino, Giuseppe;Rossi, Elisabetta [Synthesis,2005,# 17,art. no. Z07705SS,p. 2881 - 2886]